HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → Epiandrosterone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 3beta-Acetoxy-5alpha-androstan-17-one | HCID 908740 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Epiandrosterone | HCID 441302 | 95% |
Reaktionsschritte
A mixture of 5 (1 g, 3.00 mmol), NaOH 0.12 g (3.44 mmol) in methanol was refluxed for 10 min, cooled to room temperature and treated with water. The resulting precipitate was filtered off and washed with water to afford crude product 6 (0.82 g, 95%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08623849B2 |
| Quelldatensatz | uspto-grants-2014_01 |
| ORD ID | ord-ae5f46f7bef043fb87e21b3a77341060 |
| Quellennotiz | uspto-grants-2014_01 |