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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 47531Erstellt: 24. Oktober 2026

Hydroxyacetone → 2-Propanone, 1-((methylsulfonyl)oxy)-

https://huagongshe.com/de/reaction/47531

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydroxyacetoneHCID 8299—
EduktMethanesulfonyl chlorideHCID 31297—
EduktSodium BicarbonateHCID 516892—
LösungsmittelChloroformHCID 6212—
Produkt2-Propanone, 1-((methylsulfonyl)oxy)-HCID 146754—

Reaktionsschritte

Thirty-seven (37) mg of hydroxyacetone was dissolved in 2 ml of chloroform, and to which 0.078 ml of methanesulfonyl chloride was added. After stirring the reaction liquid at room temperature for 30 minutes, saturated aqueous sodium bicarbonate solution was added and extracted with chloroform. The extract was dried over anhydrous sodium sulfate and concentrated to provide the title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06699880B1
Quelldatensatzuspto-grants-2004_03
ORD IDord-ae0dc196daec479296ba40aa26395f87
Quellennotizuspto-grants-2004_03