HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 2-Amino-1-phenoxy-propene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | p-Toluenesulfonic acid | HCID 6101 | — |
| Edukt | 1-Phenoxy-2-propanone | HCID 69313 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 2-Amino-1-phenoxy-propene | HCID 70048860 | — |
Reaktionsschritte
0.2 mol of phenoxyacetone in 200 ml of tetrahydrofuran is saturated at reflux temperature with ammonia gas with the addition of 0.2 g of p-toluene sulphonic acid. The mixture is allowed to stand at room temperature for 24 hours and the solvent is then removed by evaporation in vacuo. The evaporation residue is employed crude in the reaction of Example 5B.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04886804 |
| Quelldatensatz | uspto-grants-1989_12 |
| ORD ID | ord-f9508f221bf3480cacb1d5f539bc49be |
| Quellennotiz | uspto-grants-1989_12 |