HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(4aS,8aR)-4-(3,4-Diethoxyphenyl)-2-[1-(toluene-4-sulfonyl)-piperidin-4-yl]-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one → HCID 23396188, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (4aS,8aR)-4-(3,4-Diethoxyphenyl)-2-[1-(toluene-4-sulfonyl)-piperidin-4-yl]-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one | HCID 10175016 | — |
| Edukt | Isonicotinoyl chloride hydrochloride | HCID 12262826 | — |
| Produkt | HCID 23396188 | HCID 23396188 | — |
Reaktionsschritte
Prepared from isonicotinoyl chloride hydrochloride and starting compound A2 as described for compound 1. After evaporating the dichloromethane solution, the residue is dissolved in diethyl ether. After addition of a saturated solution of hydrochloric acid in ether, the titel compound precipitates. M.p. 66-68° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07531540B2 |
| Quelldatensatz | uspto-grants-2009_05 |
| ORD ID | ord-78f9c1e6663446aeae02aab230e9b07e |
| Quellennotiz | uspto-grants-2009_05 |