HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(S)-(+)-2-Phenylglycine amide → 2-Amino-2-phenylacetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (S)-(+)-2-Phenylglycine amide | HCID 729986 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2-Amino-2-phenylacetamide | HCID 12791 | — |
Reaktionsschritte
In accordance with the process described in JP Patent Application Laying Open (Kokai) No. 62-55097, Enterobacter cloacae N-7901 (FERM BP-873) was cultured. This culture solution, 100 mL, was centrifuged, and the wet cells were then suspended in distilled water to prepare a 270 g cell suspension. D, L-phenylglycine amide, 30 g, was dissolved in this suspension, and the mixture was then allowed to react at 40° C. for 18 hours. After the reaction, cells were removed by centrifugation and 295 g of an aqueous solution containing 5.0% by mass each of L-phenylglycine and D-phenylglycine amide was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06949658B2 |
| Quelldatensatz | uspto-grants-2005_09 |
| ORD ID | ord-6d343bb9ea194e9dab7172539ee081ee |
| Quellennotiz | uspto-grants-2005_09 |