HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Nitro-n-[1-(4-pyridyl)piperidin-4-ylmethyl]pyridine-2-amine → N2-[1-(4-pyridyl)piperidin-4-ylmethyl]-2,3-pyridinediamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Nitro-n-[1-(4-pyridyl)piperidin-4-ylmethyl]pyridine-2-amine | HCID 23497755 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Produkt | N2-[1-(4-pyridyl)piperidin-4-ylmethyl]-2,3-pyridinediamine | HCID 12150690 | 97,1% |
Reaktionsschritte
Using a similar procedure to that described in Example 2, Part C, 3-nitro-N-[1-(4-pyridyl)piperidin-4-ylmethyl]pyridine-2-amine (340 mg, 1.09 mmol) and 10% palladium on carbon (200 mg) yielded 300 mg of the title compound, which was used without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06710057B2 |
| Quelldatensatz | uspto-grants-2004_03 |
| ORD ID | ord-03bbc50c157749ee9b5b92ccfd8c784d |
| Quellennotiz | uspto-grants-2004_03 |