HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenol → 4'-Phenoxyacetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenol | HCID 996 | — |
| Edukt | Dimethylacetamide | HCID 31374 | — |
| Produkt | 4'-Phenoxyacetophenone | HCID 236783 | — |
Reaktionsschritte
4-Phenoxyacetophenone was prepared by refluxing 4-fluoroaceotone and phenol in DMAc for 16 hours. The solvent was removed under reduced pressure and the reside subjected to standard ethyl acetate/water work-up and the resulting material purified by silica gel chromatography.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07772260B2 |
| Quelldatensatz | uspto-grants-2010_08 |
| ORD ID | ord-2336461666234a08953253d8164eb22e |
| Quellennotiz | uspto-grants-2010_08 |