HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methyl-1-pentanol → 2-Methyl-1-pentyl methanesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methyl-1-pentanol | HCID 7745 | — |
| Edukt | Methanesulfonyl chloride | HCID 31297 | — |
| Produkt | 2-Methyl-1-pentyl methanesulfonate | HCID 22486761 | — |
Reaktionsschritte
The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (856 mg, 89%) from 2-methyl-1-pentanol (497 mg, 4.90 mmol) and methanesulfonyl chloride (821 mg, 7.30 mmol). 1H NMR (CDCl3, 300 MHz) δ0.89-0.93 (m, 3H), 0.98 (d, 3H, J=6.6 Hz), 1.15-1.43 (m, 4H), 1.88-1.90 (m, 1H), 3.00 (s, 3H), 3.98-4.11 (m, 2H) ppm.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06713471B1 |
| Quelldatensatz | uspto-grants-2004_03 |
| ORD ID | ord-d79780d30ecc47f799ce5e10fbff2fe1 |
| Quellennotiz | uspto-grants-2004_03 |