HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Methyl-1-pentanol → HCID 22736017, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Methyl-1-pentanol | HCID 12296 | — |
| Edukt | Methanesulfonyl chloride | HCID 31297 | — |
| Produkt | HCID 22736017 | HCID 22736017 | — |
Reaktionsschritte
The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (620 mg, 63%) from 4-methyl-1-pentanol (511 mg, 5.00 mmol) and methanesulfonyl chloride (844 mg, 7.50 mmol). 1H NMR (CDCl3, 300 MHz) δ0.88 (d, 6H, J=4.7 Hz), 1.23-1.31 (m, 2H), 1.53-1.62 (m, 1H), 1.70-1.80 (m, 2H), 3.00 (s, 3H), 4.21 (t, 2H, J=6.6 Hz) ppm.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06713471B1 |
| Quelldatensatz | uspto-grants-2004_03 |
| ORD ID | ord-eb37cb96c3ac4a40b1d317c93abe9152 |
| Quellennotiz | uspto-grants-2004_03 |