Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 51010Erstellt: 24. Oktober 2026

Acetic acid, (1,3-dihydro-2H-inden-2-ylidene)-, ethyl ester → Ethyl 2-(2,3-dihydro-1H-inden-2-yl)acetate

https://huagongshe.com/de/reaction/51010

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetic acid, (1,3-dihydro-2H-inden-2-ylidene)-, ethyl esterHCID 10631946—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthyl AcetateHCID 8857—
ProduktEthyl 2-(2,3-dihydro-1H-inden-2-yl)acetateHCID 1010435994%

Reaktionsschritte

To a solution of ethyl 1,3-dihydro-2H-inden-2-ylideneacetate (302 mg, 1.49 mmol) in EtOAc (10 mL) was added 5% Pd/C (76 mg) and H2 was bubbled through the slurry for 20 h. The slurry was then filtered through Celite and the organic solution was concentrated in vacuo. Ethyl 2,3-dihydo-1H-inden-2-ylacetate (285 mg, 94%) was isolated as a colorless oil without purification.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06713471B1
Quelldatensatzuspto-grants-2004_03
ORD IDord-a54f5142b7224ac08d0149ff911a7335
Quellennotizuspto-grants-2004_03