HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
tert-butyl N-(4-chlorophenyl)carbamate → (2-Amino-5-chloro-phenyl)-(2-chloro-6-fluoro-phenyl)-methanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | tert-butyl N-(4-chlorophenyl)carbamate | HCID 546372 | — |
| Edukt | 2-Chloro-6-fluorobenzoyl chloride | HCID 2736547 | — |
| Produkt | (2-Amino-5-chloro-phenyl)-(2-chloro-6-fluoro-phenyl)-methanone | HCID 67505353 | 42% |
Reaktionsschritte
In a manner similar to that described above for compound 1aa, 4-Chloro-N-Boc-aniline and 2-chloro-6-fluoro-benzoyl chloride were converted to 1ab (42% yield) MS m/z=284 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09102678B2 |
| Quelldatensatz | uspto-grants-2015_08 |
| ORD ID | ord-d25e6dcecf4342d29476108ff3b63072 |
| Quellennotiz | uspto-grants-2015_08 |