HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dihydrocoumarin → 4-Hydroxy-1-indanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dihydrocoumarin | HCID 660 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Produkt | 4-Hydroxy-1-indanone | HCID 590547 | — |
Reaktionsschritte
4-Hydroxy-1-indanone (76) was synthesized by aluminum chloride induced re-cyclization of dihydrocumarin (75), according to Org. Lett., 2007, 9(15), p. 2915-2918. The reaction was performed on 100 g of (75) to furnish (76) with 85% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09108916B2 |
| Quelldatensatz | uspto-grants-2015_08 |
| ORD ID | ord-07f7d30e0d48480a86a96aa16b53371a |
| Quellennotiz | uspto-grants-2015_08 |