HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Isocyanatothiophene → HCID 86636352, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Isocyanatothiophene | HCID 2776375 | — |
| Edukt | 6-Chloro-12-(2-piperidin-4-ylethoxy)-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaene tris(trifluoroacetate) | HCID 86636347 | — |
| Produkt | HCID 86636352 | HCID 86636352 | 20% |
Reaktionsschritte
The desired compound was prepared according to the procedure of Example D41 using 6-chloro-12-(2-piperidin-4-ylethoxy)-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaene tris(trifluoroacetate) and 2-isocyanatothiophene as the starting materials in 20% yield. LCMS for C29H31ClN7O2S (M+H)+: m/z=576.0.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08871753B2 |
| Quelldatensatz | uspto-grants-2014_10 |
| ORD ID | ord-592d221c20514208ac115943cd602f03 |
| Quellennotiz | uspto-grants-2014_10 |