HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 54735Erstellt: 24. Oktober 2026
1-Octanethiol → 3,4,4-trifluoro-3-butenethioic acid, S-octyl ester
https://huagongshe.com/de/reaction/54735
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1-Octanethiol | HCID 8144 | — |
| Edukt | 3,4,4-Trifluoro-3-butenoyl chloride | HCID 10920789 | — |
| Produkt | 3,4,4-trifluoro-3-butenethioic acid, S-octyl ester | HCID 15239192 | 91,3% |
Reaktionsschritte
A mixture of 3,4,4-trifluoro-3-butenoyl chloride (1.7 g, 0.0107 mole) and 1-octanethiol (0.72 g, 0.0049 mole) is heated at 70° C. for 12 h. The crude product is purified by passing through a short column of silica gel to give 1.2 g of the desired product as a pale yellow oil, a 91% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05623084 |
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| Quelldatensatz | uspto-grants-1997_04 |
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| ORD ID | ord-eb0dbc9d20ca481b847892b364cfb881 |
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| Quellennotiz | uspto-grants-1997_04 |
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