HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Chloro-4-isocyanato-2-(trifluoromethyl) benzene → 1-[4-(2-Quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)urea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Chloro-4-isocyanato-2-(trifluoromethyl) benzene | HCID 2733265 | — |
| Edukt | 2-(4-Aminophenylthio)quinoline | HCID 22637130 | — |
| Produkt | 1-[4-(2-Quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)urea | HCID 18971663 | — |
Reaktionsschritte
2-(4-Aminophenylthio)quinoline (3.9 moles, 1.0 g) and 4-chloro-3-trifluoromethylphenylisocyanate (3.9 moles, 0.85 g) were reacted according to procedure A to yield the title compound, 0.8 g, 43%. Mass Spec (FD) 463. Calculated for C23H15ClF3N3OS: C, 58.29; H, 3.19; N, 8.87. Found: C, 58.56; H, 3.43; N, 9.02. M Pt 194°-195 ° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05624937 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-edef4794f6394e139c3094c299faa755 |
| Quellennotiz | uspto-grants-1997_04 |