HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,2-Dichloro-4-isothiocyanatobenzene → 1-[4-(2-Quinolylthio)phenyl]-3-(3,4-dichlorophenyl)thiourea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,2-Dichloro-4-isothiocyanatobenzene | HCID 23065 | — |
| Edukt | 2-(4-Aminophenylthio)quinoline | HCID 22637130 | — |
| Produkt | 1-[4-(2-Quinolylthio)phenyl]-3-(3,4-dichlorophenyl)thiourea | HCID 18971669 | — |
Reaktionsschritte
2-(4-Aminophenylthio)quinoline (11.9 moles, 3.0 g) and 3,4-dichlorophenylisothiocyanate (11.9 mmoles, 2.42 g) were reacted according to procedure B to yield the title compound, 360 mg, 6.6%. Mass Spec (FD) 455. Calculated for C22H15Cl2N3S2 : C, 57.90 H, 3.31; N, 9.21. Found: C, 57.86; H, 3.53; N, 9.07. m.p. 125°-126°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05624937 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-b5d135a5c74d43408848565d0bb40f3c |
| Quellennotiz | uspto-grants-1997_04 |