HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → o-Tolyl-acetyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | o-Tolylacetic acid | HCID 69519 | — |
| Produkt | o-Tolyl-acetyl chloride | HCID 2760632 | — |
Reaktionsschritte
A solution of 2.0 g of o-tolylacetic acid in 27 ml of thionyl chloride is heated at reflux for 1 hour. The volatiles are evaporated in vacuo to give a residue which is concentrated from toluene three times and dried under vacuum to give 2.1 g of the desired product as a light brown oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05624923 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-9e3ada643d264e1abb01d8e9bf8ac9c6 |
| Quellennotiz | uspto-grants-1997_04 |