HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Guanidine Hydrochloride → HCID 178478910, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Guanidine Hydrochloride | HCID 5742 | — |
| Edukt | Methyl 1-methyl-1H-indole-5-carboxylate | HCID 10679201 | — |
| Edukt | Sodium Methoxide | HCID 10942334 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 178478910 | HCID 178478910 | 68,9% |
Reaktionsschritte
The reaction was carried out in a manner similar to Example 1 except for using 1.00 g (5.29 mmol) of methyl 1-methyl-5-indolecarboxylate, 5.05 g (52.9 mmol) of guanidine hydrochloride and 50 ml of a methanol solution of 2.85 g (52.9 mmol) of sodium methoxide. Thus 0.92 g (68.9%) of 1-methyl-5-indoloylguanidine hydrochloride was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06169107A |
| Quelldatensatz | uspto-grants-2001_01 |
| ORD ID | ord-79b75a0701a94757837a47f7f0a1043e |
| Quellennotiz | uspto-grants-2001_01 |