HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic acid, (p-tolylsulfonyl)-, ethyl ester → Toluene-4-sulfonyl-hex-4-enoic acid ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic acid, (p-tolylsulfonyl)-, ethyl ester | HCID 76102 | — |
| Edukt | 4-Bromo-2-methylbut-1-ene | HCID 549585 | — |
| Produkt | Toluene-4-sulfonyl-hex-4-enoic acid ethyl ester | HCID 86586576 | — |
Reaktionsschritte
5-Methyl-2-(3-methyl-but-2-enyl)-2-(toluene-4-sulfonyl-hex-4-enoic acid ethyl ester was prepared according to general method as outlined in example 9. Starting from ethyl α-(p-tolylsulfonyl)acetate (2.9g, 10.9 mmol and 4-bromo-2-methyl butene (3.42g, 23 mmol). Yield 4.6g; tan oil; MS 379.2 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06172057B2 |
| Quelldatensatz | uspto-grants-2001_01 |
| ORD ID | ord-daf5f68e522e48b89df0acf2c6ec9d5f |
| Quellennotiz | uspto-grants-2001_01 |