HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfamide → HCID 178479209, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfamide | HCID 82267 | — |
| Edukt | 3-Chloropropionitrile hydrogen chloride | HCID 86742043 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | HCID 178479209 | HCID 178479209 | — |
Reaktionsschritte
To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04731479 |
| Quelldatensatz | uspto-grants-1988_03 |
| ORD ID | ord-3edc6a87650c40d881e2ef0137c4c5f3 |
| Quellennotiz | uspto-grants-1988_03 |