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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 5737Erstellt: 23. Oktober 2026

Potassium Carbonate → Methyl 4-amino-3-(4-chlorocinnamylamino)benzoate

https://huagongshe.com/de/reaction/5737

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
Edukt3,5-Diamino-2-methylbenzoic acidHCID 135524—
Eduktp-Chlorocinnamyl chlorideHCID 53728250—
LösungsmittelDimethylformamideHCID 6228—
ProduktMethyl 4-amino-3-(4-chlorocinnamylamino)benzoateHCID 5381363863,2%

Reaktionsschritte

5.0 g of methyl 3,4-diaminobenzoate was dissolved in 40 ml of dimethylformamide, and to the solution were added 2.07 g of potassium carbonate and 1.87 g of p-chlorocinnamyl chloride, and reaction was carried out according to the procedure in Reference Example 40, to obtain 2.0 g of the title compound as a light brown oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05245034
Quelldatensatzuspto-grants-1993_09
ORD IDord-02666c15032d4a23816abf9f01b6ac87
Quellennotizuspto-grants-1993_09