Allyl bromide → Diethyl allylphosphonate

Beteiligte Stoffe

Reaktionsschritte

Allyl bromide was treated with triethylphosphite in the absence of solvent using microwave conditions at 150° C. to give diethyl allylphosphonate. Diethyl allylphosphonate was combined with bromotrimethyl silane and subsequently quenched with methanol to afford diethyl allylphosphonic acid according to Scheme 7.

Herkunft & Nachweise