HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Stannous chloride dihydrate → (4-Fluoro-3-(trifluoromethyl)phenyl)hydrazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Stannous chloride dihydrate | HCID 61436 | — |
| Edukt | 4-Fluoro-3-(trifluoromethyl)aniline | HCID 75377 | — |
| Edukt | Sodium Nitrite | HCID 23668193 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Produkt | (4-Fluoro-3-(trifluoromethyl)phenyl)hydrazine | HCID 2774812 | 64.390% |
Reaktionsschritte
The title compound was prepared according to the procedure described in step-1 of Intermediate-61 by using 4-fluoro-3-(trifluoromethyl)aniline (3.0 g, 0.016 mmol), NaNO2 (1.73 g, 0.025 mmol), SnCl2.2H2O (9.39 g, 0.041 mmol) and conc. HCl (100 mL) to afford 2.0 g of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09439890B2 |
| Quelldatensatz | uspto-grants-2016_09 |
| ORD ID | ord-20dc6dfe4d63487aa01a19a960959ba1 |
| Quellennotiz | uspto-grants-2016_09 |