HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyldithiocarbamic acid, dimethylamine → alpha-(1-Nitroethyl)benzyl dimethyldithiocarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Edukt | (2-Nitro-2-propenyl)benzene | HCID 575754 | — |
| Lösungsmittel | Carbon Disulfide | HCID 6348 | — |
| Produkt | alpha-(1-Nitroethyl)benzyl dimethyldithiocarbamate | HCID 21324624 | — |
Reaktionsschritte
As in Example 17, reaction of (2-nitro-2-propenyl)benzene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide, gave α-(1-nitroethyl)benzyl dimethyldithiocarbamate melting at 92° C.-94° C. when recrystallized without heating from acetone-ethanol solution.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04011230 |
| Quelldatensatz | uspto-grants-1977_03 |
| ORD ID | ord-42b83970ab794375977e587eb15f3827 |
| Quellennotiz | uspto-grants-1977_03 |