HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 59866Erstellt: 24. Oktober 2026
Dimethylformamide dimethyl acetal → Methyl 4-[3-(dimethylamino)prop-2-enoyl]benzoate
https://huagongshe.com/de/reaction/59866
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Edukt | Methyl 4-acetylbenzoate | HCID 137990 | — |
| Produkt | Methyl 4-[3-(dimethylamino)prop-2-enoyl]benzoate | HCID 10561611 | — |
Reaktionsschritte
A mixture of methyl 4-acetylbenzoate (5.00 g, 28.1 mmol) in DMF-DMA (38 mL, 284 mmol) was heated at 105° C. for 20 hours. The reaction was cooled, concentrated, and used crude in the next reaction.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US09440964B2 |
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| Quelldatensatz | uspto-grants-2016_09 |
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| ORD ID | ord-8ca3e56aacc74e2aae48df2c703518c5 |
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| Quellennotiz | uspto-grants-2016_09 |
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