2-Hydroxybenzonitrile → O-2-cyanophenyl dimethylthiocarbamate

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	2-Hydroxybenzonitrile	HCID 11907	—
Edukt	Potassium Hydroxide	HCID 14797	—
Edukt	Dimethylthiocarbamoyl chloride	HCID 27871	—
Produkt	O-2-cyanophenyl dimethylthiocarbamate	HCID 14795403	94%

Reaktionsschritte

If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US05246961
Quelldatensatz	uspto-grants-1993_09
ORD ID	ord-0e3bf4991a3f466d9c41ae0105fc4554
Quellennotiz	uspto-grants-1993_09