Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Tert-butyl 2-diazoacetate | HCID 5097903 | — |
| Edukt | 3-[2-(2-Methoxyethoxy)ethoxy]prop-1-yne | HCID 18381683 | — |
| Produkt | HCID 178496244 | HCID 178496244 | — |
Reaktionsschritte
To a solution containing approx. 2.5 g 3-[2-(2-Methoxy-ethoxy)-ethoxy]-propyne, 2.8 g Diazo-acetic acid tert-butyl ester were added and the mixture was heated to 70° C. for 5 days. Then the solution was concentrated under reduced pressure and directly purified by chromatography on silica eluting with a n-heptane/ethyl acetate gradient. Yield: 1.7 g.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07910606B2 |
|---|
| Quelldatensatz | uspto-grants-2011_03 |
|---|
| ORD ID | ord-2e5006ab6c204dcf9cdbd0ebe55193eb |
|---|
| Quellennotiz | uspto-grants-2011_03 |
|---|
