HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide → HCID 178418303, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide | HCID 53937500 | — |
| Edukt | Sodium hydrogen sulphide | HCID 86586439 | — |
| Produkt | HCID 178418303 | HCID 178418303 | 65,2% |
Reaktionsschritte
Using the procedure from Preparation 34, 5.8 g (17.9 mmol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide was reacted with 5.1 g (72 mmol) of sodium hydrogen sulfide to give 3.75 g of the title compound, mp 189-193° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06001863 |
| Quelldatensatz | uspto-grants-1999_12 |
| ORD ID | ord-a835807953bf4b7ea12570979ef5341d |
| Quellennotiz | uspto-grants-1999_12 |