HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Butyn-2-ol → Undec-8-en-3-yne-2,5-diol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Butyn-2-ol | HCID 16239 | — |
| Edukt | Hept-4-enal | HCID 71590 | — |
| Edukt | HCID 178418443 | HCID 178418443 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | Undec-8-en-3-yne-2,5-diol | HCID 123300045 | — |
Reaktionsschritte
But-3-yn-2-ol was added into a solution of ethyl magnesium bromide (EtMgBr) in tetrahydrofuran (THF). Hept-4-enal was then dropped into the mixture at room temperature and aged for 2 hours. The rush over process provided the product undec-8-en-3-yne-2,5-diol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09441185B2 |
| Quelldatensatz | uspto-grants-2016_09 |
| ORD ID | ord-031d4fef6cf0407a9a44ce165221682a |
| Quellennotiz | uspto-grants-2016_09 |