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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 614019Erstellt: 24. Oktober 2026

Cyanide → 3-(m-Chloro-alpha,alpha-dimethylbenzyl)-1-methyl-1-pentylurea

https://huagongshe.com/de/reaction/614019

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktCyanideHCID 5975—
EduktN-MethylpentylamineHCID 117479—
Edukt1-Chloro-3-(2-isocyanatopropan-2-yl)benzeneHCID 21329849—
LösungsmittelHexaneHCID 8058—
Produkt3-(m-Chloro-alpha,alpha-dimethylbenzyl)-1-methyl-1-pentylureaHCID 2132984091,3%

Reaktionsschritte

A solution of 3.9 g of m-chloro-α,α-dimethylbenzyl isocyanate, prepared from the corresponding cyanide in the same way as in Synthesis Example 1, in 10 ml of n-hexane was added to 4 g of N-methyl-N-pentylamine and the mixture was allowed to stand overnight. The precipitated crystals were separated by filtration and washed thoroughly with n-hexane to obtain 5.4 g of the title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04143061
Quelldatensatzuspto-grants-1979_03
ORD IDord-6e65560c741f40138a713f3d9d87c0d8
Quellennotizuspto-grants-1979_03