HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,5-Dimethylbenzene-1,2-diol → 2,6-Dimethylhydroquinone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,5-Dimethylbenzene-1,2-diol | HCID 17737 | — |
| Edukt | Methyl ethyl ketone peroxide | HCID 3672772 | — |
| Produkt | 2,6-Dimethylhydroquinone | HCID 69560 | — |
Reaktionsschritte
By following in the same manner as in Example 56 except that 11.2 g. (P=67.7) of methyl ethyl ketone peroxide was used instead of 4-methyl-2-pentanone peroxide, 4.68 g. (33.9 m.moles) of 3,5-dimethylcatechol and 2.17 g. (15.7 m.moles) of 2,6-dimethylhydroquinone were obtained. The yield of dihydric alkylphenols was 73.3%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04072722 |
| Quelldatensatz | uspto-grants-1978_02 |
| ORD ID | ord-5e70033e1caa400a85226405e255d509 |
| Quellennotiz | uspto-grants-1978_02 |