HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 20368146, Verbindung → 1H-1,4-Benzodiazepine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 20368146 | HCID 20368146 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Lösungsmittel | Acetyl chloride | HCID 6367 | — |
| Produkt | 1H-1,4-Benzodiazepine | HCID 148431 | — |
Reaktionsschritte
In the manner given in Example 1, a solution of 8-fluoro-1-methyl-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine in dimethylformamide, N,N,N',N'-tetrapropyldiaminomethane and acetyl chloride (in 0.5 molar excess compared to the N,N,N',N'-tetrapropyldiaminomethane) are reacted together to give 8-fluoro-1[2-(dipropylamino)ethyl]-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a][1,4-benzodiazepine
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04075221 |
| Quelldatensatz | uspto-grants-1978_02 |
| ORD ID | ord-e375e263f104480eb2604e29d92efb05 |
| Quellennotiz | uspto-grants-1978_02 |