Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Nitric Acid | HCID 944 | — |
| Edukt | N-(2,4-Dimethylphenyl)acetamide | HCID 16303 | — |
| Lösungsmittel | Sulfuric Acid | HCID 1118 | — |
| Produkt | Acetamide, N-(2,4-dimethyl-5-nitrophenyl)- | HCID 112848 | — |
Reaktionsschritte
A mixture of concentrated nitric acid (20 mL) and concentrated sulfuric acid (20 mL) was cooled in an ice-salt bath to 0° C. N-(2,4-dimethylphenyl)acetamide (9.5 g) was added portionwise at such a rate to maintain the temperature below 5° C. The mixture was then allowed to stir in the cold for an additional one hour.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05952362 |
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| Quelldatensatz | uspto-grants-1999_09 |
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| ORD ID | ord-80511f65a2bb47f180d0bd088cb65e37 |
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| Quellennotiz | uspto-grants-1999_09 |
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