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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 618222Erstellt: 24. Oktober 2026

Nitric Acid → Acetamide, N-(2,4-dimethyl-5-nitrophenyl)-

https://huagongshe.com/de/reaction/618222

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktNitric AcidHCID 944—
EduktN-(2,4-Dimethylphenyl)acetamideHCID 16303—
LösungsmittelSulfuric AcidHCID 1118—
ProduktAcetamide, N-(2,4-dimethyl-5-nitrophenyl)-HCID 112848—

Reaktionsbedingungen

Temperatur0 °C

Reaktionsschritte

A mixture of concentrated nitric acid (20 mL) and concentrated sulfuric acid (20 mL) was cooled in an ice-salt bath to 0° C. N-(2,4-dimethylphenyl)acetamide (9.5 g) was added portionwise at such a rate to maintain the temperature below 5° C. The mixture was then allowed to stir in the cold for an additional one hour.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05952362
Quelldatensatzuspto-grants-1999_09
ORD IDord-80511f65a2bb47f180d0bd088cb65e37
Quellennotizuspto-grants-1999_09