HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(3-Bromopropoxy)-3-nitrobenzene → 3-(3-Bromopropoxy)-aniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(3-Bromopropoxy)-3-nitrobenzene | HCID 7172301 | — |
| Katalysator | Nickel | HCID 935 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 3-(3-Bromopropoxy)-aniline | HCID 459256 | — |
Reaktionsschritte
1 g of Raney nickel is added to a solution of 4 g of 3-(3-bromopropoxy)-nitrobenzene in 40 ml of tetrahydrofuran and the starting substance is hydrogenated at room temperature. The catalyst is filtered off and washed with tetrahydrofuran. Evaporation of the filtrate gives 3-(3-bromopropoxy)-aniline as a colourless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04820726 |
| Quelldatensatz | uspto-grants-1989_04 |
| ORD ID | ord-6f3552bc1fe14ba992e508f19b21d72c |
| Quellennotiz | uspto-grants-1989_04 |