HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Bromo-2-chloro-6-methylpyridine → HCID 90202624, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Bromo-2-chloro-6-methylpyridine | HCID 2734418 | — |
| Edukt | 3-Oxetanone | HCID 15024254 | — |
| Produkt | HCID 90202624 | HCID 90202624 | 71% |
Reaktionsschritte
In analogy to the procedure described in Example 130 a), 3-bromo-2-chloro-6-methylpyridine (CAN 185017-72-5, 5 g, 24.2 mmol) was reacted with oxetan-3-one (CAN 6704-31-0, 1.75 g, 1.42 mL, 24.2 mmol) to give the title compound (3.42 g, 71%) as off-white solid, MS (ESI): m/e=200.5 [MH+].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09303012B2 |
| Quelldatensatz | uspto-grants-2016_04 |
| ORD ID | ord-6e94af4091a6499abe54c42ce8a01fc4 |
| Quellennotiz | uspto-grants-2016_04 |