HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-[(2-Nitrophenyl)sulfanyl]benzoic acid → 2-((2-Aminophenyl)thio)benzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-[(2-Nitrophenyl)sulfanyl]benzoic acid | HCID 376978 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | 2-((2-Aminophenyl)thio)benzoic acid | HCID 10955828 | — |
Reaktionsschritte
To a solution of 2-((2-nitrophenyl)thio)benzoic acid, prepared as described in the previous step, (43.3 g, 0.157 mol) in ethyl acetate (500 mL) was added Pd/C (8 g). The reaction solution was stirred at room temperature overnight under hydrogen gas atmosphere. The mixture was filtered and concentrated to provide the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09304126B2 |
| Quelldatensatz | uspto-grants-2016_04 |
| ORD ID | ord-91e47b447afe49b2be3082fc09c284fa |
| Quellennotiz | uspto-grants-2016_04 |