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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 625174Erstellt: 24. Oktober 2026

2-[(2-Nitrophenyl)sulfanyl]benzoic acid → 2-((2-Aminophenyl)thio)benzoic acid

https://huagongshe.com/de/reaction/625174

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-[(2-Nitrophenyl)sulfanyl]benzoic acidHCID 376978—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthyl AcetateHCID 8857—
Produkt2-((2-Aminophenyl)thio)benzoic acidHCID 10955828—

Reaktionsschritte

To a solution of 2-((2-nitrophenyl)thio)benzoic acid, prepared as described in the previous step, (43.3 g, 0.157 mol) in ethyl acetate (500 mL) was added Pd/C (8 g). The reaction solution was stirred at room temperature overnight under hydrogen gas atmosphere. The mixture was filtered and concentrated to provide the title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09304126B2
Quelldatensatzuspto-grants-2016_04
ORD IDord-91e47b447afe49b2be3082fc09c284fa
Quellennotizuspto-grants-2016_04