HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Iodobenzoic acid → HCID 89907118, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Iodobenzoic acid | HCID 12060 | — |
| Edukt | 3-Fluoro-4-(trifluoromethoxy)aniline | HCID 19436618 | — |
| Produkt | HCID 89907118 | HCID 89907118 | — |
Reaktionsschritte
The title compound was prepared in an analogous fashion to that described in Stage 30.1 using 3-iodobenzoic acid and 3-fluoro-4-(trifluoromethoxy)aniline to afford the title compound as a white solid. UPLC-MS (Condition 1) tR=3.39 min, m/z=425.9 [M+H]+, m/z=423.9 [M−H]−; 1H-NMR (400 MHz, DMSO-d6) δ ppm 7.32-7.40 (m, 1H) 7.54-7.62 (m, 1H) 7.64 (dd, 1H) 7.93-8.01 (m, 3H) 8.29 (s, 1H) 10.64 (s, 1H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09315489B2 |
| Quelldatensatz | uspto-grants-2016_04 |
| ORD ID | ord-213804908a0c44128c284fa57ce5542d |
| Quellennotiz | uspto-grants-2016_04 |