HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 86674754, Verbindung → 2-Amino-2-ethyl-N-methyl-butyramide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 86674754 | HCID 86674754 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | 2-Amino-2-ethyl-N-methyl-butyramide | HCID 79810370 | 75% |
Reaktionsschritte
A mixture of tert-butyl 3-(methylcarbamoyl)pentan-3-ylcarbamate (0.18 g, 0.74 mmol) in 10 ml saturated hydrochloride in ethyl acetate was stirred for 60 min at room temperature. Then the solution was evaporated to dryness to obtain the product (80 mg, 75%) as a light yellow solid; MS (LC/MS): 145.2 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09321727B2 |
| Quelldatensatz | uspto-grants-2016_04 |
| ORD ID | ord-c87266b78f9b4f709056706310a5c905 |
| Quellennotiz | uspto-grants-2016_04 |