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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 632113Erstellt: 24. Oktober 2026

6-Cyclopentenyl-pyridine-2-carboxylic acid → 6-Cyclopentyl-pyridine-2-carboxylic acid

https://huagongshe.com/de/reaction/632113

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt6-Cyclopentenyl-pyridine-2-carboxylic acidHCID 86674758—
EduktHCID 178418361HCID 178418361—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
Produkt6-Cyclopentyl-pyridine-2-carboxylic acidHCID 8667475999,6%

Reaktionsschritte

A mixture of 6-cyclopentenyl-pyridine-2-carboxylic acid (0.08 g, 0.42 mmol) and palladium on carbon (10% w/w, 0.04 g, 0.3 mmol) in ethanol (10 mL) was charged with a hydrogen balloon and stirred at room temperature overnight. The reaction mixture was filtered and the filtrate was concentrated to obtain the crude product as white solid (0.08 g, 99%) which was used directly in the next step without further purification; MS (EI): m/e=192.2 [M+H]+.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09321727B2
Quelldatensatzuspto-grants-2016_04
ORD IDord-4d38f164c2e245a5a609904cdc05383f
Quellennotizuspto-grants-2016_04