HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Cyclopentenyl-pyridine-2-carboxylic acid → 6-Cyclopentyl-pyridine-2-carboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Cyclopentenyl-pyridine-2-carboxylic acid | HCID 86674758 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 6-Cyclopentyl-pyridine-2-carboxylic acid | HCID 86674759 | 99,6% |
Reaktionsschritte
A mixture of 6-cyclopentenyl-pyridine-2-carboxylic acid (0.08 g, 0.42 mmol) and palladium on carbon (10% w/w, 0.04 g, 0.3 mmol) in ethanol (10 mL) was charged with a hydrogen balloon and stirred at room temperature overnight. The reaction mixture was filtered and the filtrate was concentrated to obtain the crude product as white solid (0.08 g, 99%) which was used directly in the next step without further purification; MS (EI): m/e=192.2 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09321727B2 |
| Quelldatensatz | uspto-grants-2016_04 |
| ORD ID | ord-4d38f164c2e245a5a609904cdc05383f |
| Quellennotiz | uspto-grants-2016_04 |