HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Fluorobenzaldehyde → 4-Fluorobenzoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Edukt | 3-Chloro-4-fluorobenzoyl Chloride | HCID 2736548 | — |
| Produkt | 4-Fluorobenzoyl chloride | HCID 67879 | — |
Reaktionsschritte
This object is achieved by a process for the preparation of 3-chloro-4-fluorobenzoyl chloride. It comprises reacting 4-fluorobenzaldehyde with a chlorinating agent in the presence of a free-radical initiator in the presence or absence of a solvent at from −20 to 200° C. to give 4-fluorobenzoyl chloride, and reacting the 4-fluorobenzoyl chloride with a chlorinating agent in the presence of a chlorination catalyst in the presence or absence of a solvent at from −20 to 200° C. to give 3-chloro-4-fluorobenzoyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06187952B1 |
| Quelldatensatz | uspto-grants-2001_02 |
| ORD ID | ord-31cc3ee68c6545349a557221c4de7ed5 |
| Quellennotiz | uspto-grants-2001_02 |