HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(2S)-2-[[2-(3,5-difluorophenyl)acetyl]amino]propanoic acid → HCID 178501428, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (2S)-2-[[2-(3,5-difluorophenyl)acetyl]amino]propanoic acid | HCID 12135350 | — |
| Edukt | HCID 178419105 | HCID 178419105 | — |
| Lösungsmittel | Dichloromethane methanol | HCID 21226129 | — |
| Produkt | HCID 178501428 | HCID 178501428 | — |
Reaktionsschritte
Following General Procedure A and using N-(3,5-difluorophenylacetyl)-L-alanine (from Example B2) and L-histidine methyl ester dihydrochloride (Sigma), the title compound was prepared as a solid (mp=195-197° C.). The reaction was monitored by tlc (Rf=0.29 in 10% CH3OH/CH2Cl2).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06191166B1 |
| Quelldatensatz | uspto-grants-2001_02 |
| ORD ID | ord-fde0312b335f4ca8ae2fe279155cb55f |
| Quellennotiz | uspto-grants-2001_02 |