HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3-one → 17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3beta-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3-one | HCID 13020886 | — |
| Edukt | Lithium tri-tert-butoxyaluminohydride | HCID 16710494 | — |
| Produkt | 17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3beta-ol | HCID 70360261 | 64,7% |
Reaktionsschritte
1.0 g of 17β-acetoxy-1α-methyl-17α-n-propyl-5α-androstan-3-one is reacted as described in Example 6 with lithium tri-tert.-butoxyaluminum hydride and worked up. After chromatography on silica gel, 650 mg of 17β-acetoxy-1α-methyl-17α-n-propyl-5α-androstan-3β-ol is obtained as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04558041 |
| Quelldatensatz | uspto-grants-1985_12 |
| ORD ID | ord-c57fb37166684883a243a0c987bdbe6f |
| Quellennotiz | uspto-grants-1985_12 |