HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hex-4-en-3-one → (+/-)-6-(4,5-Dihydro-3-ethyl-5-methyl-1-pyrazoly)-4-trifluoromethylquinolin-2(1H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hex-4-en-3-one | HCID 17244 | — |
| Edukt | 6-(4,5-Dihydro-3-methyl-1-pyrazoly)-4-trifluoromethylquinolin-2(1H)-one | HCID 67156328 | — |
| Produkt | (+/-)-6-(4,5-Dihydro-3-ethyl-5-methyl-1-pyrazoly)-4-trifluoromethylquinolin-2(1H)-one | HCID 67156931 | — |
Reaktionsschritte
This compound was prepared from the condensation of Compound 793 (Structure 159 of Scheme XXXIII) and 2-hexen-4-one as yellow solid. 1H NMR (500 MHz, DMSO-d6) 12.1 (bs, 1H), 7.41 (dd, J=8.8, 2.4, 1H), 7.34 (d, J=8.8, 1H), 7.21 (bs, 1H), 6.92 (s, 1H), 4.37-4.28 (m, 1H), 3.12 (dd, J=17.1, 10.2, 1H), 2.53 (dd, J=17.1, 4.9, 1H), 2.37 (q, J=7.3, 2H), 1.12 (t, J=7.3, 3H), 1.12 (d, J=5.9, 3H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07696246B2 |
| Quelldatensatz | uspto-grants-2010_04 |
| ORD ID | ord-c54760aac088497ca2f3079d6fd3b3d2 |
| Quellennotiz | uspto-grants-2010_04 |