HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Picolinic acid → 2-Pyridinecarboxylic acid, sodium salt (1:1)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Picolinic acid | HCID 1018 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Katalysator | Zinc Carbonate | HCID 19005 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2-Pyridinecarboxylic acid, sodium salt (1:1) | HCID 23668608 | — |
Reaktionsschritte
An aqueous solution of sodium picolinate was prepared from 12.3 grams (100 mmol) of picolinic acid, about 4 grams of sodium hydroxide, and 50 ml of water while adjusting the solution to pH 7.2 with an amount of NaOH. With stirring, 2.84 grams (25 mmol of Zn2+) of basic zinc carbonate, 3Zn(OH)2.2ZnCO3.H2O was added to the solution. The resulting mixture indicated pH 13.8.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04740363 |
| Quelldatensatz | uspto-grants-1988_04 |
| ORD ID | ord-3e99a2973ad8469c92d405500958f5bf |
| Quellennotiz | uspto-grants-1988_04 |