HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 2-bromo-4,5,6,7-tetrahydro-N-(2-mercapto-4-methylphenyl)-benzo[b]thiophene-3-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 2-Amino-5-methylbenzene-1-thiol | HCID 323260 | — |
| Edukt | 2-Bromo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylic acid | HCID 18422137 | — |
| Produkt | 2-bromo-4,5,6,7-tetrahydro-N-(2-mercapto-4-methylphenyl)-benzo[b]thiophene-3-carboxamide | HCID 18422305 | — |
Reaktionsschritte
In the same manner as in Starting Material Synthesis Example 60 and using 2-bromo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylic acid, thionyl chloride and 2-amino-5-methylthiophenol, 2-bromo-4,5,6,7-tetrahydro-N-(2-mercapto-4-methylphenyl)-benzo[b]thiophene-3-carboxamide is obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06271225B1 |
| Quelldatensatz | uspto-grants-2001_08 |
| ORD ID | ord-c7805cf493b84872a17584f5c9f16dcf |
| Quellennotiz | uspto-grants-2001_08 |