HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenacyl bromide → alpha-(4-Chloro-2-naphthoxy)acetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenacyl bromide | HCID 6259 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 4-Chloro-1-naphthol | HCID 11787 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | alpha-(4-Chloro-2-naphthoxy)acetophenone | HCID 20563338 | — |
Reaktionsschritte
The product of step A is reacted with α-bromoacetophenone in benzene in the presence of potassium carbonate using the method of Example 1, step A, to provide white crystals of α-(4-chloro-2-naphthoxy)acetophenone after recrystallization from a dichloromethane-petroleum ether mixture.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04128659 |
| Quelldatensatz | uspto-grants-1978_12 |
| ORD ID | ord-bf48fa7d40fa410cb77be9c23de72d02 |
| Quellennotiz | uspto-grants-1978_12 |