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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 66356Erstellt: 24. Oktober 2026

Pyridine → N-(3-(Oxazolo[4,5-b]pyridin-2-yl)phenyl)acetamide

https://huagongshe.com/de/reaction/66356

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPyridineHCID 1049—
EduktAcetic AnhydrideHCID 7918—
Edukt3-(Oxazolo[4,5-b]pyridin-2-yl)anilineHCID 611086—
LösungsmittelWaterHCID 962—
ProduktN-(3-(Oxazolo[4,5-b]pyridin-2-yl)phenyl)acetamideHCID 2995970—

Reaktionsschritte

A solution of 0.63 g. of 2-(3-aminophenyl)oxazolo[4,5-b]pyridine in 10 ml. of pyridine was treated with 0.35 ml. of acetic anhydride with stirring. After stirring over the weekend the mixture was diluted to 50 ml. with water. After stirring a short time and cooling, the precipitate was collected, washed with water and dried. Recrystallization from ethyl acetate gave 2-(3-acetamidophenyl)oxazolo[4,5-b]pyridine, m.p. 201.5-202.5.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04131677
Quelldatensatzuspto-grants-1978_12
ORD IDord-c8282c7f83c448a3bc9223f140a8bc7b
Quellennotizuspto-grants-1978_12