HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
cis-4-(3-Chlorophenyl)-but-3-enylamine → 4-(3-Chlorophenyl)butan-1-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | cis-4-(3-Chlorophenyl)-but-3-enylamine | HCID 58679830 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Platinum dioxide monohydrate | HCID 11139377 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-(3-Chlorophenyl)butan-1-amine | HCID 10655071 | 74,2% |
Reaktionsschritte
A solution of cis-4-(3-chlorophenyl)-but-3-enylamine (1.2 g) in 20 mL methanol was added to platinum(IV) oxide monohydrate (0.12 g). The mixture was stirred under 1 atm of hydrogen for 16 h. The mixture was filtered through celite, and the methanol was removed in vacuo to yield 0.9 g of 4-(3-chlorophenyl)-butylamine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07084154B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-6eda0c359052479e89b251fa31711b9d |
| Quellennotiz | uspto-grants-2006_08 |