HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tert-butyl 1,4-diazepane-1-carboxylate → 4-(4-Amino-2-methoxyphenyl)-[1,4]diazepane-1-carboxylic acid tert-butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tert-butyl 1,4-diazepane-1-carboxylate | HCID 2756058 | — |
| Edukt | 1-Fluoro-2-methoxy-4-nitrobenzene | HCID 14451968 | — |
| Produkt | 4-(4-Amino-2-methoxyphenyl)-[1,4]diazepane-1-carboxylic acid tert-butyl ester | HCID 68987937 | — |
Reaktionsschritte
According to methods E and F 1-Fluoro-2-methoxy-4-nitro-benzene was reacted with [1,4]Diazepane-1-carboxylic acid tert-butyl ester and then the obtained nitro compound was hydrogenated. In this way the product was obtained with molecular weight 321.42 (C17H27N3O3); MS (ESI): 322 (M+H+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08822495B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-46ebcc912ded4a09b955b2dfa48c94fb |
| Quellennotiz | uspto-grants-2014_09 |