Diethylamine → 3-Bromo-n,n-diethylpropanamide

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A mixture of 3-bromopropanoyl chloride (1.0 g, 5.8 mmol) and diethylamine (1.9 g, 26 mmol) in THF (20 ml) was stirred at 0° C. for 30 min, the resulting white solid was filtered and the filtrate was concentrated to give a crude oil which was used in the next reaction without further purification.

Herkunft & Nachweise